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Creators/Authors contains: "Bhavna Sharma, Zi-Ling Xue"

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  1. (, Wuji huaxue xuebao)
    Reaction of CCl4 with zirconium amide guanidinate Zr(NMe2)2[iPrNC(NMe2)NiPr]2 (1) has been found to give ZrCl(NMe2)[iPrNC(NMe2)NiPr]2 (2) as an intermediate and later ZrCl2[iPrNC(NMe2)NiPr]2 (3). The reaction is likely radical in nature. Complex 2 has been independently prepared from the reaction of ZrCl(NMe2)3 with 2 equiv of diisopropylcarbodiimide, iPr-N=C=N-iPr, and characterized by NMR and elemental analysis. 
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